SESAME
ID09-MS/XPD

X-ray powder diffraction is a nondestructive technique widely used for the characterization of micro-crystalline materials. The method can be applied for phase identification, quantitative analysis, atomic structural determinations, and the characterization of microstructural properties such structure imperfections, domain size, stress and strain, in research fields ranging from material engeneering to chemistry, physics and archeometry.

Beamline Energy Resolution
2 [eV] @ 10000 [eV]
Beamline Energy Range
5 - 25 [keV]
Max Flux On Sample
1 * 1013 [ph/s] @ 10 [keV]
Photon Sources

W61

Type
Wiggler
Deflection Parameter K
7.8
Total Power
6 * 103 [W]
Number Of Periods
33
Period
60.5 [mm]
Monochromators

DCM

Energy Range
5 - 25 [keV]
Type
Si(111) Double Crystal Monochromator with sagittaly bent 2nd crystal.
Other Optics

Collimating Mirror

Description
Rh coated, 1.0 mt long cylindrical mirror, Dynamically Bended to 5-11 km radius
optical surface facing up

Refocusing Mirror

Description
Rh coated, 1.0 mt long cylindrical mirror, Dynamically Bended to 5-11 km radius
optical surface facing down
Endstations or Setup

Diffractometer

Diffractometer
2-circle diffractometer, with motorised translation stage to align the capillary spinner.
Detectors Available
Dectris Pilatus 300K

Sample

Sample Type
Powder
Mounting Type
Capillary

Techniques usage

Diffraction / Powder diffraction
Transmission mode with sample in capillary.

Sample Environment

Temperature
300 - 1300 [K]

Sample Holders

Description
500 rpm
Detectors

Dectris Pilatus 300K

Type
Si 2D pixel detector
Pixel Size
X = 172 [um], Y = 172 [um]
Array Size
X = 487 [pixel], Y = 619 [pixel]
Thickness
450 [um]
Passive or Active (Electronics)
Active
Dynamic Range
2 * 106 [counts/s]

Detection

Detected Particle
Photon
contacts
Mahmoud Abdellatief
Techniques
Diffraction
  • Powder diffraction
Disciplines
Chemistry
  • Catalysis
  • Electrochemistry
  • Green Chemistry
  • Other - Chemistry
  • Physical Chemistry
  • Technique Development - Chemistry
  • Theoretical Chemistry
Earth Sciences & Environment
  • Ecosystems & Biodiversity
  • Geology
  • Global change & Climate observation
  • Marine science/Oceanography
  • Mineralogy
  • Natural disaster, Desertification & Pollution
  • Other - Earth Sciences & Environment
  • Technique Development - Earth Sciences & Environment
Energy
  • Fusion
  • Other - Energy
  • Sustainable energy systems
  • Technique Development - Energy
Engineering & Technology
  • Aeronautics
  • Detectors
  • Nanotechnology & production processes
  • Other - Engineering & Technology
  • Space
  • Technique Development - Engineering & Technology
  • Transport
Humanities
  • Arts
  • Cultural Heritage
  • History
  • Other - Humanities
  • Technique Development - Humanities
Life Sciences & Biotech
  • Biophysics
  • Medicine
  • Pharmaceutics (drug screening)
  • Technique Development - Life Sciences & Biotech
Material Sciences
  • Knowledge based multifunctional materials
  • Metallurgy
  • Other - Material Sciences
  • Technique Development - Material Sciences
Physics
  • Astronomy/Astrophysics/Astroparticles
  • Hard condensed matter - structures
  • Matter under extreme conditions, warm dense matter, plasmas
  • Nanophysics & physics of confined matter
  • Other - Physics
  • Soft condensed matter physics
  • Surfaces, interfaces and thin films
  • Technique Development - Physics
control/Data analysis
Control Software Type
  • custom EIPCS-based GUI
Data Output Type
  • 1-D and 2-D diffraction patterns
Data Output Format
  • ascii (xy, gsas), tiff
Softwares For Data Analysis
  • GSAS-II, FullProf